Are, can you talk about the process of how you made these? How did you make sure your measure was accurate? Have some shed and have been thinking about making these, but haven't thought through how to do this. The rifle that likes 110 grains would be a bigger hunk of shed...
The way I see it, and how I go about it depending on what I have to work with for antler, is that there are two options for determining volume of the measure.
On smaller antler pieces I drill as deep as I can then redrill as wide as the shape of the antler will allow. Then use a different sizes of rat tail files and tapered half round files to make the hole as big as I feel comfortable with as far as wall thickness is concerned. And to shape the opening to look nice and pour well. Then, I test it buy comparing it to an adjustable measure. What it is, it is. I could at this point make it hold less buy cutting off and reshaping the open end.
On larger pieces I sometimes might do the same, make it as large as possible then trim it back.
If you have multiple pieces of antler to choose from, and want a specific volume, another method is to match the hole size and depth of your adjustable measure. Off the top of my head, I think the diameter of the hole in my brass adjustable measure is 3/8". Inset the measure at the desired charge, place the 3/8" drill bit point down in the adjustable measure and wrap masking tape around it where it meets the top of the measure marking the depth. Then I choose a piece of antler that will allow that size hole to be drilled into it leaving the smallest amount of wall thickness possible. I usually drill a tiny bit deeper to give myself a little extra at the top edge to shape the edges, form a slight pouring lip, and finish it off smooth.
Of course there is good old try and try again. Make a hole, test it for volume, hoping it is too small, and keep making it bigger a little at a time and retesting. I have some fine corn cob polishing media that is very similar to the 3f powder I usually use so I do most of my testing with that until I'm basically down to finishing work. Before I started using the media I kept a small bit of powder in a tiny pistol flask that was only used for testing the volume of measures. Test powder went back into it, not back into a container of powder that would be used for shooting.